4CH1

Elements, Compounds and Mixtures

Principles of Chemistry · 2 question types

Exam Frequency Analysis

Past paper frequency (2018 to 2024)

This topic accounts for approximately 5% of your exam marks.

stable
Rare
Stable5%

Definitions and separation techniques tested consistently across both papers.

  • In everyday English, "pure" usually means clean or natural
  • In chemistry, a pure substance = a sample containing only one element or only one compound, with nothing else present
  • "Pure" supermarket water is not chemically pure: it contains dissolved minerals, dissolved oxygen, sometimes fluoride
  • Chemically pure water contains only H₂O molecules

Testing purity by melting and boiling behaviour

  • : sharp, fixed melting point and boiling point
    • Pure water melts at 0 °C, boils at 100 °C
    • Pure NaCl melts at 801 °C
  • or impure substance: melts over a range of temperatures, not at a single value
    • Impurities lower the melting point and raise the boiling point
  • Quality control for pharmaceuticals and foodstuffs routinely uses melting-point analysis
    • A capillary tube of the sample is heated slowly in a melting-point apparatus
    • Measured value is compared against the literature value
    • Closer to the literature value, and narrower range = purer
Exam tip

Physical test to confirm a liquid is pure water

What comes up: Describe or state a physical test to show a colourless liquid is pure water (2 marks).

Write (two marks): (1) Measure its boiling point. (2) A pure sample will boil at exactly 100 °C. Alternatively: measure the freezing point and confirm it is exactly 0 °C — but you must match the stated value to the stated property.

Watch out: Chemical tests (anhydrous copper sulfate turns blue, cobalt chloride paper turns pink) identify water but do not show it is pure. The question asks for a physical test of purity, so the physical boiling/freezing-point answer is required.